Renee K. Takesue Pamela L. Campbell-Swarzenski 20251211 comma-delimited text data release DOI:10.5066/P13QWYFV Pacific Coastal and Marine Science Center, Santa Cruz, California U.S. Geological Survey https://doi.org/10.5066/P13QWYFV Renee K. Takesue Leticia P. Hallas Pamela L. Campbell-Swarzenski Nancy G. Prouty Amy E. East 2025 data release DOI:10.5066/P13QWYFV Pacific Coastal and Marine Science Center, Santa Cruz, CA U.S. Geological Survey Suggested Citation: Takesue, R.K., Hallas, L.P., Campbell-Swarzenski, P.L., Prouty, N.G., and East, A.E., 2025, Compositions of ash, soil, sediment, water, and biota after the 2020 CZU Lightning Complex Wildfire, Santa Cruz Mountains, CA: U.S. Geological Survey data release, https://doi.org/10.5066/P13QWYFV https://doi.org/10.5066/P13QWYFV Seventy-six parent and alkylated polycyclic aromatic hydrocarbons (PAHs) were quantified in wildfire ash (airborne and in situ), stream sediment, steelhead, crayfish, and marine mussels after the August 2020 CZU Lightning Complex Wildfire and at regular intervals over three years. PAHs are created by incomplete combustion of organic matter during wildfires and characteristic PAH ratios in sedimentary records are used to reconstruct fire histories. The CZU Wildfire provided a unique opportunity to quantify PAH concentrations immediately post-fire and subsequent changes over three years, identify wildfire signatures in parent PAHs and substituted (alkylated) PAHs to broaden the scope of wildfire studies and determine whether wildfire PAHs were taken up by stream and marine biota. Additional information about the field activity or activities from which these data were derived is available online at: http://cmgds.marine.usgs.gov/fan_info.php?fan=2020-638-FA Any use of trade, product, or firm names is for descriptive purposes only and does not imply endorsement by the U.S. Government. 20200912 20250313 Airborne ashes were collected up to one month post-fire. In situ ashes were collected at 6-month intervals for three years post-fire. Stream sediments were collected after first flush, high flow, and low flow conditions for three years post-fire. Marine mussels were collected in February after high flows and in June or July after low flows for three years. Steelhead and crayfish were collected in May, June, and July for two years, and PAHs were measured in Year 1 biota. Complete None planned -122.3957 -122.0342 37.3259 36.5757 USGS Metadata Identifier USGS:4c0a958c-7254-4eb1-bf0f-1b3aa160038c ISO 19115 Topic Category geoscientificInformation environment Data Categories for Marine Planning Substrate USGS Thesaurus geochemistry soil chemistry fires Marine Realms Information Bank (MRIB) keywords stream watershed sediment geochemistry environmental chemistry None U.S. Geological Survey USGS Coastal and Marine Hazards and Resources Program CMHRP Pacific Coastal and Marine Science Center PCMSC Geographic Names Information System (GNIS) Santa Cruz Mountains Ben Lomond Mountain San Gregorio Creek Pescadero Creek Butano Creek Gazos Creek Waddell Creek Scott Creek Big Creek Little Creek San Vicente Creek Santa Cruz No access constraints USGS-authored or produced data and information are in the public domain from the U.S. Government and are freely redistributable with proper metadata and source attribution. Please recognize and acknowledge the U.S. Geological Survey as the originator(s) of the dataset and in products derived from these data. U.S. Geological Survey, Pacific Coastal and Marine Science Center PCMSC Science Data Coordinator mailing and physical

2885 Mission Street

Santa Cruz CA 95060 831-427-4747 pcmsc_data@usgs.gov pic_Beach_black%20carbon.JPG Black carbon on a Santa Cruz beach after the 2020 CZU Wildfire. Photo credit: Ferdinand Oberle JPEG SGS AXYS Analytical Services Ltd., Sidney, BC, measured PAHs, percent moisture, and percent lipids. Angela Tan analyzed total organic carbon content at the USGS Pacific Coastal and Marine Science Center Sediment and Carbon Laboratory. Geochemical data are tabulated in comma separated variable (CSV) format. POLYCYCLIC AROMATIC HYDROCARBONS (PAHs): Quality Assurance (QA) measures for PAHs included external calibration curves, internal standards, lab blanks, and spiked matrix samples. All raw data are shown without censorship with corresponding QA flags and definitions. K-flagged values represent maximum possible concentrations. Percent recovery acceptance criteria in spiked matrix samples for the 16 priority PAHs were 70-130 percent except for Fluorene, which was 60-140 percent, and 50-150 percent for other PAHs. No formal logical consistency tests were conducted. Data set is complete The stated accuracy from the manufacturer for the Garmin handheld GPS used to record sediment collection locations is 3 feet. SAMPLE COLLECTION. Stream sediment was collected by hand from recently deposited fine-grained material on stream banks with solvent-cleaned stainless steel sampling tools and stored in pre-combusted amber glass jars. Ash, soil, and mixed samples were collected from undisturbed forest sites by hand with solvent-cleaned stainless steel sampling tools, stored in combusted 500 milliliter glass jars, and sieved to remove particles greater than 2 mm in diameter. 20230816 TOTAL ORGANIC CARBON CONTENT. Carbon analysis was performed at the PCMSC Carbon Laboratory by combustion, acidification, and coulometric detection using a UIC CM5015 Coulometer. Ash and sediment were dried overnight at 80 degrees Celsius and pulverized by hand in a mortar and pestle. 20 milligrams of material for total carbon (TC) were combusted at 950 degrees Celsius (UIC CM 5230 furnace) and quantified with a coulometric titration. 20 milligrams of material for total inorganic carbon (TIC) were digested with perchloric acid (UIC CM 5130 acid digester) and quantified with a coulometric titration. Total organic carbon (TOC) was calculated as the difference between TC and TIC. Average values of process duplicates are reported. 20250313 Angela Tan U.S. Geological Survey, Pacific Coastal and Marine Science Center Physical Scientist mailing and physical

2885 Mission Street

Santa Cruz CA 95060 831-460-7409 atan@usgs.gov PARENT AND ALKYLATED POLYCYCLIC AROMATIC HYDROCARBON (PAH) CONCENTRATIONS, PERCENT MOISTURE, PERCENT LIPID: 76 parent and alkylated polycyclic aromatic hydrocarbons (PAHs) were analyzed at SGS AXYS Analytical Services Ltd. (AXYS), a ultra-trace laboratory, by their extended PAH method. Samples were spiked with surrogate standards, Soxhlet-extracted with dichloromethane, and cleaned up with column chromatography and activated copper. PAHs were quantified by isotope dilution low resolution gas chromatography mass spectrometry in multiple ion detection mode to acquire data for target analytes and paired surrogates to minimize false positive identifications. Sample-specific concentration Reporting Limits (RL) for every analyte are reported for every quantified analyte. Due to the wide range of values in environmental samples, PAH concentrations are reported with three significant figures (XXX, XX.X, X.XX, 0.XXX, etc.) rather than a fixed measurement resolution. Percent moisture and percent lipids are ancillary parameters included with PAH analyses. 20240905 Sean Campbell SGS AXYS Analytical Services Ltd. Project Manager physical

2045 Mills Road West

Sidney BC V8L 5X2 250-655-5834 250-655-5811 sean.campbell@sgs.com Point Point 165 0.0001 0.0001 Decimal degrees D_WGS_1984 WGS_1984 6378137.0000 298.2572 CZUallPAHs_ash_sediment_biota_data.csv Table of data. PAH concentrations are formatted in scientific notation because data are reported with three significant figures for concentrations ranging several orders of magnitude. Abbreviations: OK, value meets all quality control criteria; D, dilution; J, concentration less than lowest calibration standard; K, peak detected but did not meet quantification criteria and the reported value is the maximum possible concentration; B, analyte was measured in the lab blank and in the sample; U, not detected at reporting limit; NQ, not quantified. Flag codes separated by a comma indicate more than one condition applies. -9999, not determined or not detected at reporting limit for U-flagged values. Producer defined Lab_ID Unique sample identifier for the CZU Wildfire Project (CZU) with sample type abbreviations: SED, stream sediment; HVAC, intake vent filter on the roof of PCMSC; CONTROL, unburnt forest; ASH, wildfire ash; mussel, whole body composite of Mytilus californianus from Waddell Beach; fish, whole body composite of steelhead (Oncorhynchus mykiss) from lower Scott Creek; crayfish, soft tissue composite of Pacifastacus leniusculus 88-118 millimeters in length from upper reaches of streams; AXYS_blank, lab blank specific to a sample work group. Producer defined Unique alphanumeric field sample identifier SiteID_Loc_Period Unique sample identifier assigned during field collection based on the Site (SiteID), location within the site (Loc) if relevant, and period of collection (Period). Abbreviations: VIC, San Vicente Creek; LIT, Little Creek; BIG, Big Creek; SCO, Scott Creek; WAD, Waddell Creek; GAZ, Gazos Creek; BUT, Butano Creek; PESC, Pescadero Creek; GREG, San Gregorio Creek; CONTROL, unburnt forest site; CLE, Clear Creek basin; JAM, Jamison Creek basin; LOCK, Lockheed gate; EAG, Eagle Mountain trail head; Y1, Year 1 from August 2020 to July 2021; Y2, Year 2 from August 2021 to July 2022; Y3, Year 3 from August 2022 to August 2023; PF, pre-flush; FF, first flush; HF, high flow; LF, low flow; AC, roof-top HVAC unit and number; WADsmall, mussels 40-50 millimeters in length; WADmedium, mussels 50-60 millimeters in length; WADlarge, mussels 60-70 millimeters in length; SCOsmall, fish 43-63 millimeters fork length; SCOmedium, fish 95-120 millimeters fork length; SCOlarge, fish 150-162 millimeters fork length. Producer defined Unique alphanumeric field sample identifier Date_collected Date the sample was collected, in mm/dd/yy. -9999=not applicable Producer defined 09/12/20 08/16/23 mm/dd/yy 1 Latitude_WGS84 Latitude where the sample was collected relative to geodetic datum WGS84. -9999=not applicable Producer defined 36.5757 37.3259 decimal degrees 0.0001 Longitude_WGS84 Longitude where the sample was collected relative to geodetic datum WGS84. Producer defined -122.3957 -122.0342 decimal degrees 0.0001 AXYS_WorkGroup Identifier assigned to a batch of samples by SGS AXYS Analytical Services Ltd. SGS AXYS Analytical Services Ltd. Unique alphanumeric batch identifier AXYS_SampleID Unique identifier assigned to each sample by SGS AXYS Analytical Services Ltd. SGS AXYS Analytical Services Ltd. Unique alphanumeric sample identifier Sample_weight Amount of material extracted for PAH analysis. Sediment and ash weights are dry weights. Fish, crayfish, and mussel weights are wet weights. Producer defined 3.13 15.00 grams 0.01 PercentMoisture Moisture content of material extracted for PAH analysis, in percent. -9999=not determined Producer defined 0.0 85.5 percent 0.1 PercentLipid Lipid content of material extracted for PAH analysis, in percent. -9999=not determined Producer defined 0.48 5.00 percent 0.01 PercentTOC Total organic carbon (TOC) content of bulk ash and sediment, in percent. -9999=not determined Producer defined 0.29 12.14 percent 0.01 Naphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.11E-1 2.48E+3 nanograms per gram (ng/g) Naphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Naphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.30E-3 3.63E+0 nanograms per gram (ng/g) Acenaphthylene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.50E-2 2.41E+2 nanograms per gram (ng/g) Acenaphthylene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Acenaphthylene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 5.10E-3 7.93E-1 nanograms per gram (ng/g) Acenaphthene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.30E-2 6.59E+1 nanograms per gram (ng/g) Acenaphthene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Acenaphthene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 8.90E-3 1.45E+0 nanograms per gram (ng/g) 2-Methylfluorene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.50E-2 5.76E+1 nanograms per gram (ng/g) 2-Methylfluorene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2-Methylfluorene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.70E-3 1.39E+0 nanograms per gram (ng/g) C2-Phenanthrenes/Anthracenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.40E-2 9.81E+2 nanograms per gram (ng/g) C2-Phenanthrenes/Anthracenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Phenanthrenes/Anthracenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.50E-3 9.55E-1 nanograms per gram (ng/g) Fluorene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.30E-2 1.78E+2 nanograms per gram (ng/g) Fluorene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Fluorene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.20E-3 6.99E-1 nanograms per gram (ng/g) Phenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. Flag codes separated by a comma (,) indicate multiple conditions apply. -9999=not detected when U-flagged or not determined Producer defined 4.40E-2 1.45E+3 nanograms per gram (ng/g) Phenanthrene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Phenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.40E-3 2.42E+0 nanograms per gram (ng/g) Anthracene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.20E-2 1.88E+2 nanograms per gram (ng/g) Anthracene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Anthracene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.30E-3 5.46E-1 nanograms per gram (ng/g) C1-Phenanthrenes/Anthracenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.00E-2 1.13E+3 nanograms per gram (ng/g) C1-Phenanthrenes/Anthracenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard` Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Phenanthrenes/Anthracenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.40E-3 8.38E-1 nanograms per gram (ng/g) Fluoranthene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. Producer defined 2.40E-2 6.55E+2 nanograms per gram (ng/g) Fluoranthene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Fluoranthene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.10E-3 6.88E-1 nanograms per gram (ng/g) Pyrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.50E-2 5.07E+2 nanograms per gram (ng/g) Pyrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Pyrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.00E-3 6.80E-1 nanograms per gram (ng/g) Benz[a]anthracene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 5.00E-3 1.17E+2 nanograms per gram (ng/g) Benz[a]anthracene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Benz[a]anthracene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 3.60E-3 8.23E-1 nanograms per gram (ng/g) Chrysene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.00E-2 4.51E+2 nanograms per gram (ng/g) Chrysene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Chrysene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.10E-3 8.76E-1 nanograms per gram (ng/g) Benzo[b]fluoranthene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. Flag codes separated by a comma (,) indicate multiple conditions apply. -9999=not detected when U-flagged or not determined Producer defined 1.20E-2 2.33E+2 nanograms per gram (ng/g) Benzo[b]fluoranthene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Benzo[b]fluoranthene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.10E-3 1.31E+0 nanograms per gram (ng/g) Benzo[j,k]fluoranthenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.20E-2 2.01E+2 nanograms per gram (ng/g) Benzo[j,k]fluoranthenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Benzo[j,k]fluoranthenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 8.30E-3 1.47E+0 nanograms per gram (ng/g) Benzo[e]pyrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.80E-2 2.26E+2 nanograms per gram (ng/g) Benzo[e]pyrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Benzo[e]pyrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.09E-2 1.98E+0 nanograms per gram (ng/g) Benzo[a]pyrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.90E-2 1.10E+2 nanograms per gram (ng/g) Benzo[a]pyrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Benzo[a]pyrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.17E-2 2.04E+0 nanograms per gram (ng/g) Perylene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.60E-2 5.45E+1 nanograms per gram (ng/g) Perylene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Perylene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.17E-2 2.05E+0 nanograms per gram (ng/g) Dibenz[a,h]anthracene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.00E-2 2.55E+1 nanograms per gram (ng/g) Dibenz[a,h]anthracene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Dibenz[a,h]anthracene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.40E-3 2.18E+0 nanograms per gram (ng/g) Indeno[1,2,3-cd]pyrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.30E-2 1.37E+2 nanograms per gram (ng/g) Indeno[1,2,3-cd]pyrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Indeno[1,2,3-cd]pyrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.07E-2 2.21E+0 nanograms per gram (ng/g) Benzo[ghi]perylene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.20E-2 2.30E+2 nanograms per gram (ng/g) Benzo[ghi]perylene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Benzo[ghi]perylene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.03E-2 1.94E+0 nanograms per gram (ng/g) 2-Methylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 6.10E-2 8.83E+2 nanograms per gram (ng/g) 2-Methylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2-Methylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.20E-3 1.22E+0 nanograms per gram (ng/g) 1-Methylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.60E-2 6.22E+2 nanograms per gram (ng/g) 1-Methylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1-Methylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.70E-3 1.28E+0 nanograms per gram (ng/g) C1-Naphthalenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 7.20E-2 1.51E+3 nanograms per gram (ng/g) C1-Naphthalenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Naphthalenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.20E-3 1.22E+0 nanograms per gram (ng/g) Biphenyl_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 5.00E-2 1.30E+3 nanograms per gram (ng/g) Biphenyl_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Biphenyl_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.50E-3 1.79E+0 nanograms per gram (ng/g) C1-Biphenyls_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.70E-2 1.02E+2 nanograms per gram (ng/g) C1-Biphenyls_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Biphenyls_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.40E-3 7.92E-1 nanograms per gram (ng/g) C2-Biphenyls_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 5.30E-2 1.03E+2 nanograms per gram (ng/g) C2-Biphenyls_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Biphenyls_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.90E-3 2.70E+0 nanograms per gram (ng/g) C2-Naphthalenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.67E-1 1.59E+3 nanograms per gram (ng/g) C2-Naphthalenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Naphthalenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.71E-2 2.32E+0 nanograms per gram (ng/g) 1,2-Dimethylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.10E-2 1.56E+2 nanograms per gram (ng/g) 1,2-Dimethylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1,2-Dimethylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.71E-2 1.92E+0 nanograms per gram (ng/g) 2,6-Dimethylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.60E-2 2.68E+2 nanograms per gram (ng/g) 2,6-Dimethylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2,6-Dimethylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.42E-2 1.40E+0 nanograms per gram (ng/g) C3-Naphthalenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 5.90E-2 1.01E+3 nanograms per gram (ng/g) C3-Naphthalenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C3-Naphthalenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 8.10E-3 2.34E+0 nanograms per gram (ng/g) 2,3,6-Trimethylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.70E-2 1.08E+2 nanograms per gram (ng/g) 2,3,6-Trimethylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2,3,6-Trimethylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.90E-3 2.31E+0 nanograms per gram (ng/g) 2,3,5-Trimethylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.30E-2 3.11E+2 nanograms per gram (ng/g) 2,3,5-Trimethylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2,3,5-Trimethylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 8.20E-3 4.43E+0 nanograms per gram (ng/g) C4-Naphthalenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.40E-2 3.13E+2 nanograms per gram (ng/g) C4-Naphthalenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C4-Naphthalenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.90E-3 1.71E+0 nanograms per gram (ng/g) C1-Acenaphthenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.00E-2 6.91E+1 nanograms per gram (ng/g) C1-Acenaphthenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Acenaphthenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.20E-3 1.17E+0 nanograms per gram (ng/g) C1-Fluorenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 7.70E-2 2.35E+1 nanograms per gram (ng/g) C1-Fluorenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Fluorenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.70E-3 1.39E+0 nanograms per gram (ng/g) 1,7-Dimethylfluorene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.60E-2 1.71E+1 nanograms per gram (ng/g) 1,7-Dimethylfluorene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1,7-Dimethylfluorene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.29E-2 1.27E+0 nanograms per gram (ng/g) C2-Fluorenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.20E-2 1.77E+2 nanograms per gram (ng/g) C2-Fluorenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Fluorenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.29E-2 1.33E+0 nanograms per gram (ng/g) C3-Fluorenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.80E-2 1.35E+2 nanograms per gram (ng/g) C3-Fluorenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C3-Fluorenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.11E-2 1.64E+0 nanograms per gram (ng/g) Dibenzothiophene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 9.00E-3 2.91E+1 nanograms per gram (ng/g) Dibenzothiophene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Dibenzothiophene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.00E-3 6.16E-1 nanograms per gram (ng/g) C1-Dibenzothiophenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.60E-2 2.28E+1 nanograms per gram (ng/g) C1-Dibenzothiophenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Dibenzothiophenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 8.40E-3 6.16E-1 nanograms per gram (ng/g) 2/3-Methyldibenzothiophenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.60E-2 7.71E+0 nanograms per gram (ng/g) 2/3-Methyldibenzothiophenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2/3-Methyldibenzothiophenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 8.40E-3 9.82E-1 nanograms per gram (ng/g) C2-Dibenzothiophenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.70E-2 6.36E+1 nanograms per gram (ng/g) C2-Dibenzothiophenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Dibenzothiophenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.90E-3 1.17E+0 nanograms per gram (ng/g) 2,4-Dimethyldibenzothiophene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.50E-2 4.38E+0 nanograms per gram (ng/g) 2,4-Dimethyldibenzothiophene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2,4-Dimethyldibenzothiophene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.50E-3 4.38E+0 nanograms per gram (ng/g) 4,6-Dimethyldibenzothiophene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 6.00E-3 6.86E+0 nanograms per gram (ng/g) 4,6-Dimethyldibenzothiophene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 4,6-Dimethyldibenzothiophene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 5.80E-3 1.00E+0 nanograms per gram (ng/g) C3-Dibenzothiophenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.80E-2 3.63E+1 nanograms per gram (ng/g) C3-Dibenzothiophenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C3-Dibenzothiophenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.40E-3 1.23E+0 nanograms per gram (ng/g) C4-Dibenzothiophenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 6.10E-2 1.41E+1 nanograms per gram (ng/g) C4-Dibenzothiophenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C4-Dibenzothiophenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.40E-3 5.91E-1 nanograms per gram (ng/g) 3-Methylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.00E-2 1.52E+2 nanograms per gram (ng/g) 3-Methylphenanthrene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 3-Methylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.50E-3 8.59E-1 nanograms per gram (ng/g) 2-Methylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.40E-2 3.34E+2 nanograms per gram (ng/g) 2-Methylphenanthrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2-Methylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.70E-3 9.19E-1 nanograms per gram (ng/g) 2-Methylanthracene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.70E-2 7.11E+1 nanograms per gram (ng/g) 2-Methylanthracene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2-Methylanthracene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.40E-3 8.26E-1 nanograms per gram (ng/g) 9/4-Methylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.30E-2 1.47E+2 nanograms per gram (ng/g) 9/4-Methylphenanthrene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 9/4-Methylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.50E-3 8.59E-1 nanograms per gram (ng/g) 1-Methylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.10E-2 4.30E+2 nanograms per gram (ng/g) 1-Methylphenanthrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1-Methylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 9.40E-3 8.38E-1 nanograms per gram (ng/g) 3,6-Dimethylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.80E-2 5.62E+1 nanograms per gram (ng/g) 3,6-Dimethylphenanthrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 3,6-Dimethylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.60E-3 9.78E-1 nanograms per gram (ng/g) 2,6-Dimethylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.30E-2 4.34E+1 nanograms per gram (ng/g) 2,6-Dimethylphenanthrene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 2,6-Dimethylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.50E-3 9.55E-1 nanograms per gram (ng/g) 1,7-Dimethylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.50E-2 6.17E+2 nanograms per gram (ng/g) 1,7-Dimethylphenanthrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1,7-Dimethylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.40E-3 9.32E-1 nanograms per gram (ng/g) 1,8-Dimethylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 6.00E-3 2.67E+1 nanograms per gram (ng/g) 1,8-Dimethylphenanthrene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1,8-Dimethylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.50E-3 9.55E-1 nanograms per gram (ng/g) C3-Phenanthrenes/Anthracenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.80E-2 5.37E+2 nanograms per gram (ng/g) C3-Phenanthrenes/Anthracenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C3-Phenanthrenes/Anthracenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.70E-3 1.97E+0 nanograms per gram (ng/g) 1,2,6-Trimethylphenanthrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.30E-2 4.96E+1 nanograms per gram (ng/g) 1,2,6-Trimethylphenanthrene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1,2,6-Trimethylphenanthrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.70E-3 2.15E+0 nanograms per gram (ng/g) Retene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.20E-2 2.01E+3 nanograms per gram (ng/g) Retene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined Retene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.68E-2 1.07E+1 nanograms per gram (ng/g) C4-Phenanthrenes/Anthracenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.63E-1 2.44E+3 nanograms per gram (ng/g) C4-Phenanthrenes/Anthracenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined D Sample was diluted Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C4-Phenanthrenes/Anthracenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.68E-2 1.07E+1 nanograms per gram (ng/g) C1-Fluoranthenes/Pyrenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 7.00E-3 3.17E+2 nanograms per gram (ng/g) C1-Fluoranthenes/Pyrenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Fluoranthenes/Pyrenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.30E-3 1.02E+0 nanograms per gram (ng/g) 3-Methylfluoranthene/Benzo[a]fluorene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.20E-2 1.37E+2 nanograms per gram (ng/g) 3-Methylfluoranthene/Benzo[a]fluorene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 3-Methylfluoranthene/Benzo[a]fluorene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.30E-3 1.02E+0 nanograms per gram (ng/g) C2-Fluoranthenes/Pyrenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 7.00E-3 1.99E+2 nanograms per gram (ng/g) C2-Fluoranthenes/Pyrenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Fluoranthenes/Pyrenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 5.80E-3 7.27E-1 nanograms per gram (ng/g) C3-Fluoranthenes/Pyrenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.30E-2 5.95E+1 nanograms per gram (ng/g) C3-Fluoranthenes/Pyrenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C3-Fluoranthenes/Pyrenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 5.90E-3 5.59E-1 nanograms per gram (ng/g) C4-Fluoranthenes/Pyrenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.80E-2 2.46E+1 nanograms per gram (ng/g) C4-Fluoranthenes/Pyrenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C4-Fluoranthenes/Pyrenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 6.70E-3 9.61E-1 nanograms per gram (ng/g) C1-Benzo[a]anthracenes/Chrysenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 8.00E-3 4.08E+2 nanograms per gram (ng/g) C1-Benzo[a]anthracenes/Chrysenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Benzo[a]anthracenes/Chrysenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.20E-3 6.32E-1 nanograms per gram (ng/g) 5/6-Methylchrysene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.00E-2 2.55E+1 nanograms per gram (ng/g) 5/6-Methylchrysene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 5/6-Methylchrysene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.10E-3 6.24E-1 nanograms per gram (ng/g) 1-Methylchrysene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.40E-2 1.31E+2 nanograms per gram (ng/g) 1-Methylchrysene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1-Methylchrysene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.20E-3 6.40E-1 nanograms per gram (ng/g) C2-Benzo[a]anthracenes/Chrysenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.30E-2 2.10E+2 nanograms per gram (ng/g) C2-Benzo[a]anthracenes/Chrysenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Benzo[a]anthracenes/Chrysenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.90E-3 1.42E+0 nanograms per gram (ng/g) 5,9-Dimethylchrysene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.10E-2 4.71E+1 nanograms per gram (ng/g) 5,9-Dimethylchrysene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 5,9-Dimethylchrysene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.90E-3 1.42E+0 nanograms per gram (ng/g) C3-Benzo[a]anthracenes/Chrysenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.25E-1 4.07E+1 nanograms per gram (ng/g) C3-Benzo[a]anthracenes/Chrysenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C3-Benzo[a]anthracenes/Chrysenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.30E-3 9.31E-1 nanograms per gram (ng/g) C4-Benzo[a]anthracenes/Chrysenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 2.50E-2 2.21E+1 nanograms per gram (ng/g) C4-Benzo[a]anthracenes/Chrysenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C4-Benzo[a]anthracenes/Chrysenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 7.30E-3 1.25E+0 nanograms per gram (ng/g) C1-Benzofluoranthenes/Benzopyrenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 4.10E-2 2.44E+2 nanograms per gram (ng/g) C1-Benzofluoranthenes/Benzopyrenes_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C1-Benzofluoranthenes/Benzopyrenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.68E-2 1.37E+0 nanograms per gram (ng/g) 7-Methylbenzo[a]pyrene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.60E-2 2.20E+1 nanograms per gram (ng/g) 7-Methylbenzo[a]pyrene_FLAG Quality assurance (QA) code. Producer defined OK No QC flags Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 7-Methylbenzo[a]pyrene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.68E-2 1.37E+0 nanograms per gram (ng/g) C2-Benzofluoranthenes/Benzopyrenes_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 3.80E-2 8.16E+1 nanograms per gram (ng/g) C2-Benzofluoranthenes/Benzopyrenes_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined C2-Benzofluoranthenes/Benzopyrenes_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 1.62E-2 4.43E+0 nanograms per gram (ng/g) 1,4,6,7-Tetramethylnaphthalene_CONC PAH concentration in dry weight sediment, dry weight ash, or wet weight biota. -9999=not detected when U-flagged or not determined Producer defined 1.80E-2 3.43E+1 nanograms per gram (ng/g) 1,4,6,7-Tetramethylnaphthalene_FLAG Quality assurance (QA) code. Flag codes separated by a comma (,) indicate multiple conditions apply. Producer defined OK No QC flags Producer defined B Analyte found in the work group lab blank associated with the sample Producer defined J Concentration was less than the lowest calibration standard Producer defined K Analyte peak was detected but did not meet quantification criteria. The reported value is the maximum possible concentration Producer defined U Analyte was not detected at the reporting limit (RL) Producer defined NQ Analysis failed to meet QA criteria Producer defined 1,4,6,7-Tetramethylnaphthalene_RL Sample-specific reporting limit (RL) in dry weight sediment, dry weight ash, or wet weight biota. -9999=not determined Producer defined 4.90E-3 1.71E+0 nanograms per gram (ng/g) The first line of the csv file is a header line. U.S. Geological Survey U.S. Geological Survey - CMGDS mailing and physical

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Santa Cruz CA 95060 1-831-427-4747 pcmsc_data@usgs.gov These data are available in csv format (CZUallPAHs_ash_sediment_biota_data.csv), accompanied by CSDGM FGDC compliant metadata and a map on the landing page showing sample locations. Unless otherwise stated, all data, metadata and related materials are considered to satisfy the quality standards relative to the purpose for which the data were collected. Although these data and associated metadata have been reviewed for accuracy and completeness and approved for release by the U.S. Geological Survey (USGS), no warranty expressed or implied is made regarding the display or utility of the data on any other system or for general or scientific purposes, nor shall the act of distribution constitute any such warranty. comma-delimited text File contains the csv table and the associated metadata. No compression applied 0.2688 https://doi.org/10.5066/P13QWYFV Data and metadata can be downloaded using the Network_Resource_Name link and scrolling down to the Sampling Data section. None. These data can be viewed with any text reader. 20251211 U.S. Geological Survey, Pacific Coastal and Marine Science Center PCMSC Science Data Coordinator mailing and physical

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Santa Cruz CA 95060 831-427-4747 pcmsc_data@usgs.gov Content Standard for Digital Geospatial Metadata FGDC-STD-001-1998